2
votes
2answers
47 views
Glovebox best practices
As some one who has spent too much time doing air sensitive chemistry, I've always wondered what is the best practice for bringing small quantities of liquid samples into the glov …
0
votes
0answers
19 views
Best-Practices Procedure for Working with tert-Butyllithium?
The case of Sheharbano (Sheri) Sangji serves as a reminder to respect and understand the materials in a research lab. Even then, things can go wrong.
Where can I find a detailed, …
0
votes
1answer
58 views
Most-widely used, but rarely-cited papers?
What are the most widely-used, but rarely cited papers in experimental chemistry? My votes for organic synthesis would be:
Rapid chromatographic technique for preparative separat …
2
votes
1answer
48 views
Best Practices for Solvent Stills?
Continuously-operated solvent stills have been the cause of many laboratory fires in the last several years. Although alternatives exist, not every lab is willing to upgrade.
Does …
1
vote
2answers
146 views
Printable chart of cold bath temperatures?
Where can I find a good printable chart of cold bath temperatures?
It should, for example give the temperatures for various dry-ice/organic solvent mixtures, liquid nitrogen/organ …
2
votes
2answers
77 views
What are good online resources for synthetic practices and “collective wisdom?”
Besides this site (which is more interactive), I'm aware of Not Voodoo.
Are there any other good sources for beginning synthetic students?
